Microwave irradiation for 15 minutes allowed the highly selective hydrothermal synthesis of the diamagnetic, air-stable oxidation catalyst [PW11O39RuII(DMSO)](5-), as confirmed by H-1, P-31, Ru-99 and W-183 NMR techniques.
Microwave Assisted Rapid Incorporation of Ruthenium into Lacunary Keggin-Type Polyoxotungstates: One-step Synthesis, 99Ru, 183W NMR Characterization and Catalytic Activity of [PW11O39RuII(DMSO)]5-
BAGNO, ALESSANDRO;BONCHIO, MARCELLA;SARTOREL, ANDREA;SCORRANO, GIANFRANCO
2000
Abstract
Microwave irradiation for 15 minutes allowed the highly selective hydrothermal synthesis of the diamagnetic, air-stable oxidation catalyst [PW11O39RuII(DMSO)](5-), as confirmed by H-1, P-31, Ru-99 and W-183 NMR techniques.
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